Procedure: Standardization of misdirect sulphuric point 1. 1.32g of the atomic number 11 carbonate was weighted sinlessly in a beaker. 2. 120cm3 of deionised urine was added to the beaker containing sodium carbonate. 3. The mixture was displace gently to let the sodium carbonate to dissolve. 4. The dissolving agent was poured into a 250cm3 volumetrical flask. 5. The beaker was washed surface with further small quantities of water. 6. totally the washings were poured into the 250cm3 volumetric flask to secure no theme was left(p) on the wall of the beaker. 7. Water was added into the conic flask until the butt was made up by a wash bottle. 8. The solution was shaked well. 9. 25cm3 of sodium carbonate solution was pipetted pop out and ran into a conical flask. 10. Two to three drops of methyl chromatic indicator solution was added into the conical flask.. 11. A burette was fill up with the sulphuric bitter of unknown concentration. 12. The flask was swirled during the addition of dilute sulphuric acid. 13. Adding of weaken sulphuric acid was stopped when the disguise of the solution changed from yellowish to pink. 14. Step 9 to step 13 was repeated in two ways in hallow to get a more accurate result. Determination of acetylsalicylic acid in aspirin tablets/ 1. Three tablets were weighted accurately. 2.
The tablets were putted into a 250cm3. 3. 25cm3 of 1.0M sodium hydroxide was added into the conical flask by a pipette. 4. 25cm3 of deionised water was added into the flask to dilute the solution. 5. The flask was warmed over a tripod and gauze for ten minutes. 6. The rea ction mixture was cooled and transferred wit! h washings to a 250 cm3 volumetric flask. 7. 25cm3 of the solution was titrated with the standardized sulphuric acid, using phenolphthalein as an indicator, If you requirement to get a full essay, order it on our website: OrderCustomPaper.com
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